Bleach Episode 44 - “Ishida’s Ultimate Power!”

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Uryū uses the Quincy technique ransōtengai to overcome the paralysis of Mayuri’s zanpakutō. However, he is outclassed by Mayuri, and is forced to take off his sanrei glove, an act that releases the limits on his powers. Uryū proceeds to completely overwhelms Mayuri, but Mayuri escapes by transforming into a liquid. Uryū continues on towards Rukia’s cell, severely weakened, until he is confronted by another Soul Reaper captain, Kaname Tōsen.